2M55

NMR structure of the complex of an N-terminally acetylated alpha-synuclein peptide with calmodulin

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	900
2	Bruker	AVANCE	Bruker Avance	800
3	Bruker	AVANCE	Bruker Avance	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	3D 1H-15N NOESY
10	1	1	2D 1H-13C HSQC aliphatic
11	1	1	2D 1H-13C HSQC aromatic
12	1	2	2D 1H-13C HSQC aliphatic
13	1	2	2D 1H-13C HSQC aromatic
14	1	3	2D 1H-13C HSQC aliphatic
15	1	1	3D CBCA(CO)NH
2	1	2	3D 1H-15N NOESY
3	1	1	3D 1H-13C NOESY aliphatic
4	1	1	2D 1H-13C HSQC aromatic
5	1	2	3D 1H-13C NOESY aliphatic
6	1	2	3D 1H-13C NOESY aromatic
7	1	1	2D 1H-15N HSQC
8	1	2	2D 1H-15N HSQC
9	1	3	2D 1H-15N HSQC

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.36	ambient	310

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20