2LYR
NOE-based 3D structure of the monomeric partially-folded intermediate of CylR2 at 259K (-14 Celsius degrees)
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Bruker | AVANCE III | Bruker Avance III | 700 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 2D 1H-15N HSQC |
2 | 1 | 1 | 2D 1H-13C HSQC aliphatic |
3 | 1 | 1 | 2D 1H-13C HSQC aromatic |
4 | 1 | 1 | 3D 1H-13C NOESY aromatic |
5 | 1 | 1 | 3D HCCH-TOCSY |
6 | 1 | 1 | 3D 1H-13C NOESY aliphatic |
7 | 1 | 1 | 3D 1H-15N NOESY |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 7 | ambient | 259 |
Conformers
Conformers Calculated Total Number | 200 |
Conformers Submitted Total Number | 20 |