2LWZ
NMR Structures of Single-chain Insulin
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Bruker | Avance | Bruker Avance | 800 |
2 | Bruker | Avance | Bruker Avance | 700 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 2D 1H-15N HSQC |
10 | 1 | 1 | 4D Time-shared NOESY (4D-N15,C13-edited and 4D-C13,C13-edited NOESY) |
2 | 1 | 1 | 2D 1H-13C HSQC |
3 | 1 | 1 | 3D HNCACB |
4 | 1 | 1 | 3D CBCA(CO)NH |
5 | 1 | 1 | 3D HNCO |
6 | 1 | 1 | 3D C(CO)NH |
7 | 1 | 1 | 3D H(CCO)NH |
8 | 1 | 1 | 3D HCCH-TOCSY |
9 | 1 | 1 | 3D 1H-15N NOESY |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 7 | ambient | 298 |
Conformers
Conformers Calculated Total Number | 70 |
Conformers Submitted Total Number | 20 |