2LRA

NMR Structure of Signal Sequence Deleted (SSD) Rv0603 Protein from Mycobacterium tuberculosis without N-terminal His-tag

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	INOVA	Varian INOVA	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	3	2D 1H-13C HSQC aromatic
11	1	2	2D CB(CGCD)HD
12	1	2	2D CB(CGCE)HE
13	1	2	2D 1H-1H NOESY aromatic
14	1	1	3D 1H-15N NOESY
15	1	3	3D 1H-13C NOESY aliphatic
16	1	3	3D 1H-13C NOESY aromatic
2	1	2	3D HNCACB
3	1	2	3D CBCA(CO)NH
4	1	2	3D HNCO
5	1	2	3D HN(CO)CA
6	1	2	3D H(CCO)NH
7	1	2	3D C(CO)NH
8	1	2	3D HCCH-TOCSY
9	1	3	2D 1H-13C HSQC aliphatic

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.5	ambient	298

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	10