2L9Q

Structural Characterization of small heat shock protein (Hsp12)

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	INOVA	Varian INOVA	900
2	Varian	INOVA	Varian INOVA	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D 1H-15N NOESY
2	1	2	3D CBCA(CO)NH
3	1	2	3D HNCACB
4	1	2	2D 1H-13C HSQC aliphatic
5	1	2	2D 1H-13C HSQC aromatic
6	1	2	3D C(CO)NH
7	1	2	3D HBHA(CO)NH
8	1	2	3D HCCH-COSY
9	1	2	3D 1H-13C NOESY aliphatic

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	ambient	313

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20