2L5G
Co-ordinates and 1H, 13C and 15N chemical shift assignments for the complex of GPS2 53-90 and SMRT 167-207
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE | Bruker Avance | 800 |
| 2 | Bruker | DMX | Bruker DMX | 600 |
| 3 | Bruker | DRX | Bruker DRX | 500 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-15N HSQC |
| 10 | 1 | 1 | 3D HBHA(CO)NH |
| 11 | 1 | 1 | 3D HCCH-COSY |
| 12 | 1 | 1 | 3D CCH-TOCSY |
| 13 | 1 | 1 | 3D C(CO)NH |
| 14 | 1 | 1 | 3D 1H-15N NOESY |
| 15 | 1 | 1 | 3D 1H-13C NOESY aliphatic |
| 16 | 1 | 1 | 3D 1H-13C NOESY aromatic |
| 17 | 1 | 2 | 2D 1H-15N HSQC |
| 18 | 1 | 2 | 2D 1H-13C HSQC |
| 19 | 1 | 2 | 2D 1H-13C HSQC aliphatic |
| 2 | 1 | 1 | 2D 1H-13C HSQC |
| 20 | 1 | 2 | 2D 1H-1H NOESY filtered to retain only interchain cross-peaks |
| 21 | 1 | 3 | 2D 1H-15N HSQC |
| 22 | 1 | 3 | 2D 1H-13C HSQC |
| 23 | 1 | 3 | 2D 1H-13C HSQC aliphatic |
| 24 | 1 | 3 | 2D 1H-1H NOESY filtered to retain only interchain cross-peaks |
| 25 | 1 | 1 | 3D HNHAHB |
| 3 | 1 | 1 | 2D 1H-13C HSQC CT aliphatic |
| 4 | 1 | 1 | 2D 1H-13C HSQC CT aromatic |
| 5 | 1 | 1 | 2D 1H-1H NOESY |
| 6 | 1 | 1 | 2D 1H-1H NOESY (filtered to remove 15N-coupled signals in F1 and F2) |
| 7 | 1 | 1 | 3D HNCACB |
| 8 | 1 | 1 | 3D CBCA(CO)NH |
| 9 | 1 | 1 | 3D HNCACB |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.5 | ambient | 285 |
Conformers
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 35 |
