2L0F

Solution NMR structure of human polymerase iota UBM2 (P692A mutant) in complex with ubiquitin

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	700

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	1	3D HN(CA)CO
11	1	1	3D H(CCO)NH
12	1	1	3D C(CO)NH
13	1	2	2D 1H-15N HSQC
14	1	2	2D 1H-13C HSQC
15	1	2	3D CBCA(CO)NH
16	1	2	3D HNCACB
17	1	2	3D HNCO
18	1	2	3D HCCH-TOCSY
19	1	2	3D H(CCO)NH
2	1	1	2D 1H-13C HSQC
20	1	2	3D C(CO)NH
21	1	2	3D 1H-15N NOESY
22	1	2	3D 1H-13C NOESY
23	1	2	3D 1H-15N TOCSY
24	1	3	3D 15N, 13C FILTERED 13C EDITED
25	1	4	3D 15N, 13C FILTERED 13C EDITED
3	1	1	3D CBCA(CO)NH
4	1	1	3D HNCACB
5	1	1	3D HNCO
6	1	1	3D HBHA(CO)NH
7	1	1	3D HCCH-TOCSY
8	1	1	3D 1H-15N NOESY
9	1	1	3D 1H-13C NOESY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	ambient	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20