2KXF

Solution structure of the first two RRM domains of FBP-interacting repressor (FIR)

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	INOVA	Varian INOVA	800
2	Bruker	AVANCE	Bruker Avance	600
3	Bruker	AVANCE	Bruker Avance	700

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	2	3D CBCA(CO)NH
10	1	1	3D 1H-15N TOCSY
11	1	2	3D 1H-13C NOESY
12	1	2	3D 1H-13C NOESY optimised for aromatics
13	1	1	3D 1H-15N NOESY
2	1	3	3D HN(COCA)CB
3	1	2	3D HNCA
4	1	3	3D HNCA
5	1	2	3D HN(CO)CA
6	1	2	3D HNCO
7	1	3	3D HNCACB
8	1	2	3D HNCACB
9	1	2	3D HCCH-TOCSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	8	ambient	310

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20