2KUM

Solution structure of the human chemokine CCL27

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	DRX	Bruker DRX	500
2	Bruker	DRX	Bruker DRX	600
3	Bruker	DRX	Bruker DRX	800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	1	3D (H)NNH-NOESY
11	1	2	3D H(CCO)NH
12	1	2	3D C(CO)NH
13	1	2	3D HCCH-TOCSY
14	1	1	3D 1H-15N TOCSY
15	1	2	3D 1H-13C NOESY
16	1	1	2D 1H-1H NOESY
17	1	2	3D Me-H(C)CH-TOCSY
18	1	2	3D Me-(H)CCH-TOCSY
19	1	2	2D 1H-13C CT-HSQC
2	1	2	2D 1H-13C HSQC
20	1	1	3D 1H-15N NOESY
3	1	2	3D HNCO
4	1	2	3D HNCA
5	1	2	3D HN(CO)CA
6	1	2	3D HNCACB
7	1	2	3D HN(COCA)CB
8	1	2	3D HN(CA)CO
9	1	2	3D intra-HNCA

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	5.5	ambient	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	30