2KTF

Solution NMR structure of human polymerase iota UBM2 in complex with ubiquitin

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	Avance III	Bruker Avance III	700

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D HNCO
11	1	2	3D HCACO
12	1	1	3D C(CO)NH
13	1	1	3D H(CCO)NH
14	1	1	3D HCCH-TOCSY
15	1	2	3D HCCH-TOCSY
16	1	1	3D 1H-15N NOESY
17	1	2	3D 1H-15N NOESY
18	1	1	3D 1H-13C NOESY
19	1	2	3D 1H-13C NOESY
2	1	2	2D 1H-15N HSQC
20	1	1	3D HBHA(CO)NH
21	1	2	3D HBHA(CO)NH
22	1	1	3D 13C edited double-filtered
23	1	2	3D 13C edited double-filtered
3	1	1	2D 1H-13C HSQC
4	1	2	2D 1H-13C HSQC
5	1	1	3D HNCACB
6	1	2	3D HNCA
7	1	1	3D CBCA(CO)NH
8	1	2	3D CBCA(CO)NH
9	1	1	3D HNCO

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	ambient	301

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20