2KMJ

High resolution NMR solution structure of a complex of HIV-2 TAR RNA and a synthetic tripeptide in a 1:2 stoichiometry

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	900
2	Bruker	AVANCE	Bruker Avance	800
3	Bruker	AVANCE	Bruker Avance	700
4	Bruker	AVANCE	Bruker Avance	600
5	Bruker	DRX	Bruker DRX	600
6	Bruker	AVANCE	Bruker Avance	400

Experiment

experiment id	conditions id	solution id	Experiment type
1	2	1	2D 1H-15N HSQC
10	1	2	2D H(C)N
11	1	2	2D 1H-15N HSQC (2J)
12	1	2	2D 1H-13C HSQC
13	2	1	2D HNN-COSY
14	1	2	2D H5NN-COSY
15	1	2	3D forward-directed HCC-TOCSY-CCH E.COSY
16	2	1	2D 1H-15N CPMG-NOESY
2	1	2	2D 1H-13C HSQC
3	1	3	2D 1H-1H TOCSY
4	1	3	2D 1H-1H NOESY
5	1	4	2D 1H-1H NOESY
6	1	2	3D HCCH-TOCSY
7	1	2	3D HCCH-COSY
8	2	1	3D 1H-15N NOESY
9	1	2	3D 1H-13C NOESY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.2	ambient	298
2	6.2	ambient	283

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	10