2KJX

Solution structure of the extracellular domain of JTB

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	DRX	Bruker DRX	600
2	Bruker	DRX	Bruker DRX	800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D C(CO)NH
11	1	2	3D HCCH-TOCSY
12	1	2	3D 1H-15N NOESY
13	1	2	3D 1H-13C NOESY
14	1	2	3D HBHA(CO)NH
2	1	2	2D 1H-13C HSQC
3	1	3	2D 1H-1H NOESY
4	1	2	3D HNCA
5	1	2	3D CBCA(CO)NH
6	1	2	3D HNCACB
7	1	2	3D HNHA
8	1	2	3D HNHB
9	1	2	3D H(CCO)NH

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	5.6	ambient	298

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20