2KDU

Structural basis of the Munc13-1/Ca2+-Calmodulin interaction: A novel 1-26 calmodulin binding motif with a bipartite binding mode

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	DRX	Bruker DRX	600
2	Bruker	AVANCE	Bruker Avance	600
3	Bruker	AVANCE	Bruker Avance	700
4	Bruker	AVANCE	Bruker Avance	900
5	Bruker	DMX	Bruker DMX	800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	3D CBCA(CO)NH
10	1	3	2D 1H-13C HSQC
11	1	1	2D 1H-15N HSQC
12	1	2	2D 1H-15N HSQC
13	1	2	3D 1H-15N NOESY
14	1	2	3D HNCO
15	1	2	3D HN(CA)CO
16	1	2	3D HNCACB
17	1	2	3D CBCA(CO)NH
18	1	2	3D C(CO)NH
19	1	2	3D H(CCO)NH
2	1	1	3D HNCACB
20	1	2	3D HCCH-TOCSY
21	1	1	3D C(CO)NH
22	1	1	2D (IPAP)1H-15N HSQC
23	1	2	2D (IPAP)1H-15N HSQC
3	1	1	3D HNCO
4	1	1	3D HN(CA)CO
5	1	1	3D 1H-15N NOESY
6	1	1	3D H(CCO)NH
7	1	1	2D 1H-13C HSQC
8	1	3	3D 1H-13C NOESY
9	1	3	3D HCCH-TOCSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.8		308

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20