2KDK

Structure of human circadian clock protein BMAL2 C-terminal PAS domain

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D CCH-TOCSY
11	1	2	3D CCH-COSY
12	1	2	3D 1H-13C NOESY
13	1	2	3D 1H-13C NOESY aromatic
2	1	1	3D 1H-15N TOCSY
3	1	1	3D 1H-15N NOESY
4	1	2	2D 1H-15N HSQC
5	1	2	2D 1H-13C HSQC
6	1	2	3D HNCO
7	1	2	3D HNCACB
8	1	2	3D CBCA(CO)NH
9	1	2	3D HBHA(CO)NH

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	ambient	300

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	10