2KCT
Solution nmr structure of the ob-fold domain of heme chaperone ccme from desulfovibrio vulgaris. northeast structural genomics target dvr115g.
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE | 800 | |
| 2 | Varian | INOVA | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-15N HSQC |
| 10 | 1 | 1 | 3D HBHA(CO)NH |
| 11 | 1 | 1 | 3D HN(CA)CO |
| 12 | 1 | 1 | 3D C(CO)NH TOCSY |
| 13 | 1 | 1 | 3D HCCH-COSY ALIPHATIC |
| 14 | 1 | 1 | 3D HCCH- TOCSY ALIPHATIC |
| 15 | 1 | 1 | 3D (H)CCH- TOCSY ALIPHATIC |
| 16 | 1 | 1 | 3D HNHA |
| 17 | 1 | 1 | 2D 1H-15N HETNOE |
| 18 | 1 | 1 | 1D 1H-15N T1 AND T2 |
| 19 | 1 | 3 | 2D 1H-15N TROSY (for N-H RDC's) |
| 2 | 1 | 1 | 2D 1H-13C HSQC |
| 3 | 1 | 1 | 3D SIMULTANEOUS CN NOESY |
| 4 | 1 | 1 | 3D 1H-13C NOESY aromatic |
| 5 | 1 | 1 | 2D 1H-13C HSQC HIGH RES. (L/V METHYL STEREOASSIGNMENT) |
| 6 | 1 | 1 | 3D HNCO |
| 7 | 1 | 1 | 3D HN(CO)CA |
| 8 | 1 | 1 | 3D CBCA(CO)NH |
| 9 | 1 | 1 | 3D HNCACB |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 4.5 | AMBIENT | 298 |
Conformers
| Conformers Calculated Total Number | 100 |
| Conformers Submitted Total Number | 20 |
