2KA2
Solution NMR structure of BNIP3 transmembrane peptide dimer in detergent micelles with His173-Ser172 intermonomer hydrogen bond restraints
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Varian | INOVA | Varian INOVA | 800 |
| 2 | Varian | INOVA | Varian INOVA | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D CN-NOESY-HSQC |
| 10 | 1 | 1 | H(C)CH-COSY |
| 11 | 1 | 1 | (H)CCH-TOCSY |
| 12 | 1 | 1 | HBCBCGCDHD |
| 13 | 1 | 1 | HBCBCGCDCEHE |
| 2 | 1 | 1 | 3D 15N-edited NOESY-HSQC |
| 3 | 1 | 1 | 3D 13C-edited NOESY-HSQC optimized for aromatic carbon |
| 4 | 1 | 1 | half-filtered 3D CN-NOESY-HSQC |
| 5 | 1 | 1 | 2D spin-echo difference CT HSQC |
| 6 | 1 | 1 | HNHA |
| 7 | 1 | 1 | HNCA |
| 8 | 1 | 1 | CBCACONNH |
| 9 | 1 | 1 | HNCO |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 5.1 | 313 |
Conformers
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 20 |
