2K7Z

Solution Structure of the Catalytic Domain of Procaspase-8

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	700
2	Bruker	AVANCE	Bruker Avance	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	2	2D 1H-15N HSQC
10	1	2	3D 1H-15N NOESY
11	1	1	3D 1H-13C NOESY
12	1	2	HN(CACO)NH
13	1	1	3D HCCH-TOCSY
14	1	1	3D 1H-15N NOESY
2	1	1	2D 1H-13C HSQC
3	1	2	3D HNCACB
4	1	2	3D HN(COCA)CB
5	1	2	3D HNCO
6	1	2	3D HN(CA)CO
7	1	2	3D HN(CO)CG
8	1	2	3D HNCG
9	1	1	3D HCCH-COSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	8	ambient	305

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20