2K6T

Solution structure of the relaxin-like factor

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	INOVA	Varian INOVA	800
2	Varian	INOVA	Varian INOVA	500

Experiment

experiment id	conditions id	solution id	Experiment type
1	8	2	2D DQF-COSY
10	2	1	2D 1H-1H NOESY
11	3	1	2D 1H-1H NOESY
12	4	1	2D 1H-1H NOESY
13	5	1	2D 1H-1H NOESY
14	6	1	2D 1H-1H NOESY
15	7	1	2D 1H-1H NOESY
16	6	1	2D 1H-15N HSQC
17	9	2	2D 1H-13C HSQC
18	5	3	2D 1H-15N HSQC
19	5	3	2D 1H-15N HSQC-NOESY
2	9	2	2D DQF-COSY
3	6	1	2D DQF-COSY
4	9	2	2D 1H-1H TOCSY
5	6	1	2D 1H-1H TOCSY
6	9	2	2D 1H-13C HSQC
7	8	2	2D 1H-1H NOESY
8	9	2	2D 1H-1H NOESY
9	1	1	2D 1H-1H NOESY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	5		293
2	5		296
3	5		301
4	5		303
5	5		306
6	5		308
7	5		313
8			288
9			308

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20