2K5Z

Solution structure and dynamics of the apical stem-loop of Duck hepatitis B virus

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	INOVA	Varian INOVA	500
2	Varian	INOVA	Varian INOVA	600
3	Varian	INOVA	Varian INOVA	800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-1H NOESY
10	2	5	2D 1H-1H COSY
11	2	5	3D HCCH-TOCSY
12	2	5	3D HCN
2	3	2	2D 1H-1H NOESY
3	2	5	3D 1H-13C NOESY
4	1	3	2D 1H-15N HSQC
5	2	5	2D 1H-15N HSQC
6	3	2	2D 1H-13C HSQC
7	3	4	2D 1H-13C HSQC
8	2	5	2D 1H-13C HSQC
9	3	2	2D DQF-COSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.7	ambient	278
2	6.7	ambient	288
3	6.7	ambient	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	10