2K3U
Structure of the tyrosine-sulfated C5a receptor N-terminus in complex with the immune evasion protein CHIPS.
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Varian | INOVA | Varian INOVA | 600 |
2 | Varian | INOVA | Varian INOVA | 500 |
3 | Bruker | AVANCE | Bruker Avance | 900 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 2D 1H-15N HSQC |
10 | 2 | 2 | 3D HBHACBCA(CO)NH |
11 | 2 | 2 | 3D HCCH-TOCSY |
12 | 2 | 2 | 3D HCCH-TOCSY |
13 | 1 | 1 | 3D 1H-15N NOESY |
14 | 2 | 2 | 3D 1H-15N NOESY |
15 | 1 | 1 | 3D 1H-15N TOCSY |
16 | 2 | 2 | 3D 1H-13C NOESY |
17 | 2 | 2 | 3D 1H-13C NOESY |
18 | 2 | 2 | 2D 1H-1H NOESY |
19 | 2 | 2 | 2D 1H-1H TOCSY |
2 | 1 | 1 | 2D 1H-15N HSQC |
20 | 2 | 2 | 3D COCA(HN) |
21 | 2 | 2 | 3D-CNH-NOESY |
22 | 2 | 2 | 2D-HBHD aromatic |
23 | 2 | 2 | 2D-HBHE aromatic |
24 | 2 | 2 | 2D-CBHD aromatic |
25 | 2 | 2 | 2D-CBHE aromatic |
26 | 2 | 2 | 3D HNHA |
27 | 2 | 2 | 3D HNHB |
3 | 1 | 1 | 2D 1H-15N HSQC |
4 | 2 | 2 | 2D 1H-13C HSQC |
5 | 2 | 2 | 2D 1H-13C HSQC |
6 | 2 | 2 | 2D 1H-13C HSQC |
7 | 2 | 2 | 3D CBCA(CO)NH |
8 | 2 | 2 | 3D HNCACB |
9 | 2 | 2 | 3D HNCO |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 6.5 | ambient | 298 |
2 | 6.5 | ambient | 298 |
Conformers
Conformers Calculated Total Number | 130 |
Conformers Submitted Total Number | 25 |