2JZA

Solution NMR structure of nitrite reductase [NAD(P)H] small subunit from Erwinia carotovora. Northeast Structural Genomics Consortium target EwR120

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	800
2	Varian	INOVA	Varian INOVA	750

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	3	2D 1H-15N HSQC
10	1	2	3D HCCH-TOCSY aliphatic
11	1	2	3D HBHA(CO)NH
12	1	2	2D 1H-13C HSQC aromatic
13	1	2	2D 1H-13C CT-HSQC aliphatic
14	1	2	2D 1H-13C CT-HSQC aromatic
15	1	2	3D HCCH-COSY aromatic
16	1	2	2D 1Haro-15Naro LR-HSQC
17	1	1	2D 1H-13C CT-HSQC 28ms
18	1	1	2D 1H-13C CT-HSQC 56ms
2	1	3	3D HNCO
3	1	3	3D HNCACB
4	1	3	3D HNCA
5	1	3	3D CBCA(CO)NH
6	1	2	3D 1H-15N,13Cali,13Caro NOESY
7	1	2	2D 1H-15N HSQC
8	1	2	2D 1H-13C HSQC ali
9	1	2	3D HCCH-COSY aliphatic

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	5.5	ambient	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20