2JPO
NMR structure of Antheraea polyphemus pheromone-binding protein 1 at pH 4.5
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | Avance | 900 | |
| 2 | Bruker | DRX | 750 | |
| 3 | Bruker | DRX | 500 | |
| 4 | Bruker | DRX | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-15N HSQC |
| 10 | 1 | 1 | 3D 1H-15N NOESY |
| 11 | 1 | 1 | 3D 1H-15N TOCSY |
| 12 | 1 | 1 | 3D 1H-13C NOESY |
| 13 | 1 | 1 | 3D HCCH-COSY |
| 14 | 1 | 1 | 3D HN(CA)CO |
| 15 | 1 | 1 | 15N- RESOLVED |
| 16 | 1 | 1 | 1H,1H TOCSY |
| 17 | 1 | 1 | 3D_15N- SEPARATED NOESY |
| 18 | 1 | 1 | 3D_13C- SEPARATED NOESY |
| 2 | 1 | 1 | 2D 1H-13C HSQC |
| 3 | 1 | 1 | 3D CBCA(CO)NH |
| 4 | 1 | 1 | 3D C(CO)NH |
| 5 | 1 | 1 | 3D HNCO |
| 6 | 1 | 1 | 3D HNCA |
| 7 | 1 | 1 | 3D HNCACB |
| 8 | 1 | 1 | 3D H(CCO)NH |
| 9 | 1 | 1 | 3D HCCH-TOCSY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 4.5 | AMBIENT | 293 |
Conformers
| Conformers Calculated Total Number | 80 |
| Conformers Submitted Total Number | 20 |
