2JLT
Crystal structure of an RNA kissing complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-03 |
Detector | MARRESEARCH |
Spacegroup name | P 21 3 |
Unit cell lengths | 85.000, 85.000, 85.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.080 - 2.900 |
R-factor | 0.189 |
Rwork | 0.187 |
R-free | 0.22700 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.468 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | autoSHARP |
Refinement software | REFMAC (5.5.0054) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.070 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.080 | 0.380 |
Number of reflections | 10330 | |
<I/σ(I)> | 18.66 | 5.45 |
Completeness [%] | 98.9 | 96.6 |
Redundancy | 6.43 | 6.09 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | NA CITRATE 100MM, MPD 35%, pH 4.6 |