2JKX
Galactose oxidase. MatGO. Copper free, expressed in Pichia Pastoris.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 96.950, 88.520, 85.350 |
Unit cell angles | 90.00, 117.24, 90.00 |
Refinement procedure
Resolution | 38.240 - 1.840 |
R-factor | 0.167 |
Rwork | 0.163 |
R-free | 0.20100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1gog |
RMSD bond length | 0.011 |
RMSD bond angle | 1.265 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.300 | 1.900 |
High resolution limit [Å] | 1.840 | 1.840 |
Rmerge | 0.040 | 0.150 |
Number of reflections | 53734 | |
<I/σ(I)> | 12.8 | 4.1 |
Completeness [%] | 96.6 | 85.5 |
Redundancy | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.9 | 18% PEF 8000, 100MM MES PH5.9, 200MM CALCIUM ACETATE |