2JKS
Crystal structure of the the bradyzoite specific antigen BSR4 from toxoplasma gondii.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-002 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2008-03-10 |
| Detector | RIGAKU IMAGE PLATE |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 92.050, 92.050, 98.310 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.890 - 1.900 |
| R-factor | 0.24 |
| Rwork | 0.238 |
| R-free | 0.28900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1kzq |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.868 |
| Data reduction software | CrystalClear |
| Data scaling software | CrystalClear |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.600 | 1.970 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.060 | 0.500 |
| Number of reflections | 396248 | |
| <I/σ(I)> | 14.5 | 3.8 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 11.69 | 11.41 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | pH 6.5 |
