2JK9
The structure of splA-ryanodine receptor domain and SOCS box containing 1 in complex with a PAR-4 peptide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-03-29 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.523, 82.957, 38.540 |
Unit cell angles | 90.00, 104.42, 90.00 |
Refinement procedure
Resolution | 83.050 - 1.790 |
R-factor | 0.194 |
Rwork | 0.192 |
R-free | 0.24000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | A HOMOLOGY MODEL FROM PDB ENTRY 2FNJ |
RMSD bond length | 0.012 |
RMSD bond angle | 1.321 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0036) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.320 | 1.810 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmerge | 0.070 | 0.540 |
Number of reflections | 20678 | |
<I/σ(I)> | 12.64 | 1.67 |
Completeness [%] | 96.2 | 91.4 |
Redundancy | 3.48 | 3.32 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 25% PEG3350, 0.2M NACL, 0.1M BIS-TRIS PH 5.5 |