2JJH
E243 mutant of M. tuberculosis Rv3290C
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 298 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 102.885, 102.885, 97.816 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 89.090 - 2.700 |
| R-factor | 0.15237 |
| Rwork | 0.150 |
| R-free | 0.19435 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.461 |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 21.440 |
| High resolution limit [Å] | 2.700 |
| Rmerge | 0.140 |
| Number of reflections | 16720 |
| <I/σ(I)> | 8.3 |
| Completeness [%] | 99.6 |
| Redundancy | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
