2JJA
Crystal structure of GNA with synthetic copper base pair
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-11-24 |
Detector | ADSC CCD |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 18.160, 48.590, 59.870 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.300 |
R-factor | 0.126 |
Rwork | 0.124 |
R-free | 0.14800 |
Structure solution method | MAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.015 |
RMSD bond angle | 2.074 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 1.330 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.080 | 0.300 |
Number of reflections | 7095 | |
<I/σ(I)> | 20.4 | 4 |
Completeness [%] | 99.1 | 99.8 |
Redundancy | 11.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 10% MPD, 40 MM SODIUM CACODYLATE, PH=5.5, 20 MM COBALT HEXAMINE, 80 MM NACL, 20 MM MGCL2. |