2JHU
CRYSTAL STRUCTURE OF RHOGDI E154A,E155A MUTANT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-02 |
Detector | MARRESEARCH |
Spacegroup name | H 3 2 |
Unit cell lengths | 130.775, 130.775, 162.315 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 92.850 - 1.650 |
R-factor | 0.209 |
Rwork | 0.209 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bxw |
RMSD bond length | 0.011 |
RMSD bond angle | 1.421 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.710 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.070 | 0.800 |
Number of reflections | 63939 | |
<I/σ(I)> | 40.5 | 2 |
Completeness [%] | 99.0 | 90.5 |
Redundancy | 18.2 | 9.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 2.0 M AMMONIUM SULFATE 0.2 M SODIUM CHLORIDE 0.1 M SODIUM CACODYLATE PH 6.5 |