2JHS
CRYSTAL STRUCTURE OF RHOGDI K135H,K138H,K141H MUTANT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-BM |
Synchrotron site | APS |
Beamline | 22-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-11-04 |
Detector | MARRESEARCH |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 75.316, 75.316, 91.283 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 65.230 - 1.950 |
R-factor | 0.179 |
Rwork | 0.178 |
R-free | 0.20900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bxw |
RMSD bond length | 0.011 |
RMSD bond angle | 2.328 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.020 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.040 | 0.340 |
Number of reflections | 22205 | |
<I/σ(I)> | 35.6 | 4.9 |
Completeness [%] | 99.7 | 99.8 |
Redundancy | 6 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 1.4 M SODIUM CITRATE, 100 MM HEPES PH 7.5 |