2JH6

Human Thrombin Hirugen Inhibitor complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	100
Detector technology	CCD
Collection date	2002-05-09
Detector	RIGAKU CCD
Spacegroup name	C 1 2 1
Unit cell lengths	70.135, 71.683, 71.648
Unit cell angles	90.00, 100.22, 90.00

Refinement procedure

Resolution	19.980 - 2.210
R-factor	0.165
Rwork	0.163
R-free	0.19600
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.014
RMSD bond angle	1.538
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.3.0006)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.980	2.260
High resolution limit [Å]	2.200	2.200
Rmerge	0.550	0.330
Number of reflections	16566
Completeness [%]	100.0	98
Redundancy	3.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6.8		PH 6.80