2JGR
Crystal structure of YegS in complex with ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 287 |
Detector technology | CCD |
Collection date | 2005-04-23 |
Detector | MARRESEARCH |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 124.968, 124.968, 54.163 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 88.390 - 2.650 |
R-factor | 0.205 |
Rwork | 0.203 |
R-free | 0.24900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bon |
RMSD bond length | 0.022 |
RMSD bond angle | 2.072 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 88.000 |
High resolution limit [Å] | 2.650 |
Rmerge | 0.090 |
Number of reflections | 11841 |
<I/σ(I)> | 12 |
Completeness [%] | 97.1 |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |