2JG3
MtaqI with BAZ
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-04-21 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 59.404, 69.193, 114.390 |
Unit cell angles | 90.00, 92.16, 90.00 |
Refinement procedure
Resolution | 19.730 - 1.900 |
R-factor | 0.187 |
Rwork | 0.185 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1g38 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.699 |
Data reduction software | MAR |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.790 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.090 | 0.310 |
Number of reflections | 72769 | |
<I/σ(I)> | 14.62 | 4.94 |
Completeness [%] | 99.4 | 97.7 |
Redundancy | 4.522 | 2.88 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 298 | 3 MICROLITERS CRYSTALLIZATION BUFFER (10 MM TRIS/HCL, 300 MM NACL, PH 7.3) CONTAINING THE COMPLEX PLUS 1 MICROLITER RESERVOIR SOLUTION (100 MM KCL, 100 MM MGCL2, 6% ISOPROPANOL, 50 MM SODIUM CACODYLATE, PH 6.0), VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 298K |