2JDA
Structure of a pectin binding carbohydrate binding module determined in an monoclinic crystal form.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 113 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 111.205, 34.729, 86.711 |
Unit cell angles | 90.00, 120.58, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.350 |
R-factor | 0.145 |
Rwork | 0.143 |
R-free | 0.18000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.924 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.400 |
High resolution limit [Å] | 1.350 | 1.350 |
Rmerge | 0.030 | 0.260 |
Number of reflections | 56372 | |
<I/σ(I)> | 22.3 | 2 |
Completeness [%] | 89.3 | 38.6 |
Redundancy | 3.7 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |