2JD9
Structure of a pectin binding carbohydrate binding module determined in an orthorhombic crystal form.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 113 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 34.765, 42.630, 98.681 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.800 |
R-factor | 0.175 |
Rwork | 0.172 |
R-free | 0.24000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.021 |
RMSD bond angle | 1.875 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.080 | 0.350 |
Number of reflections | 12978 | |
<I/σ(I)> | 20.3 | 6.8 |
Completeness [%] | 96.2 | 53.5 |
Redundancy | 14 | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |