2JCM
Crystal structure of Human Cytosolic 5'-Nucleotidase II in complex with beryllium trifluoride
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-10-08 |
Detector | ADSC CCD |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 91.480, 128.260, 131.010 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.670 - 2.150 |
R-factor | 0.213 |
Rwork | 0.210 |
R-free | 0.26600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2j2c |
RMSD bond length | 0.019 |
RMSD bond angle | 1.759 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.3.0021) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.200 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.160 | 0.500 |
Number of reflections | 41406 | |
<I/σ(I)> | 7.14 | 3.36 |
Completeness [%] | 98.0 | 99.8 |
Redundancy | 5.2 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 1.8 M MAGNESIUM SULFATE, 0.1 M TRIS PH 8.5 |