2JAK
Human PP2A regulatory subunit B56g
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-10-07 |
Detector | ADSC CCD |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 105.800, 105.800, 82.100 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 21.470 - 2.600 |
R-factor | 0.216 |
Rwork | 0.214 |
R-free | 0.26000 |
Structure solution method | MAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.383 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SOLVE/RESOLVE |
Refinement software | REFMAC (5.3.0021) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.000 | 2.700 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.050 | 0.560 |
Number of reflections | 16638 | |
<I/σ(I)> | 30.11 | 4.7 |
Completeness [%] | 99.7 | 99.9 |
Redundancy | 13.9 | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 29% MPD 0.1M TRIS, PH 8.0 20MM L-PROLINE |