2J9B
THE CRYSTAL STRUCTURE OF CYTOCHROME C' FROM RUBRIVIVAX GELATINOSUS AT 1.5 A RESOLUTION AND PH 6.3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1999-10-10 |
Detector | MARRESEARCH |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 69.558, 69.558, 123.374 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.920 - 1.500 |
R-factor | 0.153 |
Rwork | 0.153 |
R-free | 0.17700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jaf |
RMSD bond length | 0.014 |
RMSD bond angle | 1.582 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.900 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.050 | 0.220 |
Number of reflections | 55765 | |
<I/σ(I)> | 29.8 | 8.2 |
Completeness [%] | 99.4 | 99.2 |
Redundancy | 9.8 | 15.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.3 | 2.4M AMMONIUM SULPHATE 0.1M SODIUM CITRATE PH6.3 |