2J72
alpha-glucan recognition by a family 41 carbohydrate-binding module from Thermotoga maritima pullulanase PulA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 106.429, 37.179, 57.213 |
Unit cell angles | 90.00, 112.38, 90.00 |
Refinement procedure
Resolution | 52.700 - 1.490 |
R-factor | 0.168 |
Rwork | 0.165 |
R-free | 0.23200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2j71 |
RMSD bond length | 0.021 |
RMSD bond angle | 1.944 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.810 | 1.540 |
High resolution limit [Å] | 1.490 | 1.490 |
Rmerge | 0.060 | 0.400 |
Number of reflections | 33245 | |
<I/σ(I)> | 11.9 | 2.8 |
Completeness [%] | 97.5 | 94.5 |
Redundancy | 3.97 | 3.37 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |