2J61

L-ficolin complexed to N-acetylglucosamine (forme C)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM30A
Synchrotron site	ESRF
Beamline	BM30A
Temperature [K]	100
Detector technology	CCD
Collection date	2004-04-04
Detector	MARRESEARCH
Spacegroup name	P 63
Unit cell lengths	79.591, 79.591, 172.040
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	15.000 - 2.700
R-factor	0.212
Rwork	0.207
R-free	0.29100
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1jc9
RMSD bond length	0.019
RMSD bond angle	2.043
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	AMoRE
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.390
High resolution limit [Å]	2.700
Rmerge	0.050
Number of reflections	16911
<I/σ(I)>	24.6
Completeness [%]	99.8
Redundancy	6.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1