2J58
The structure of Wza
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-11-19 |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 94.719, 215.268, 220.892 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 107.830 - 2.250 |
| R-factor | 0.19 |
| Rwork | 0.188 |
| R-free | 0.22600 |
| Structure solution method | SAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.292 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHELX |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 108.000 | 2.320 |
| High resolution limit [Å] | 2.260 | 2.260 |
| Rmerge | 0.080 | 0.350 |
| Number of reflections | 200359 | |
| <I/σ(I)> | 18.4 | 1.8 |
| Completeness [%] | 99.0 | 94.9 |
| Redundancy | 5 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
