2J4D
Cryptochrome 3 from Arabidopsis thaliana
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.298, 116.782, 135.024 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.900 |
R-factor | 0.1886 |
Rwork | 0.189 |
R-free | 0.22140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1np7 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.574 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.050 | 0.450 |
Number of reflections | 93259 | |
<I/σ(I)> | 16.4 | 2.2 |
Completeness [%] | 97.8 | 85.9 |
Redundancy | 4.47 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | 10 MG/ML PROTEIN, 85 MM NA-CITRATE PH 4.6, 170 MM NH4-ACETATE, 21.5 W/V-% PEG 4000 AND 7.5 V/V-% GLYCEROL |