2J43
Alpha-glucan recognition by family 41 carbohydrate-binding modules from streptococcal virulence factors
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X8C |
| Synchrotron site | NSLS |
| Beamline | X8C |
| Temperature [K] | 113 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 37.621, 71.420, 101.013 |
| Unit cell angles | 90.00, 89.98, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.600 |
| R-factor | 0.181 |
| Rwork | 0.179 |
| R-free | 0.21600 |
| Structure solution method | SAD |
| RMSD bond length | 0.021 |
| RMSD bond angle | 1.707 |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 37.620 | 1.660 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmerge | 0.090 | 0.480 |
| Number of reflections | 68393 | |
| <I/σ(I)> | 9.2 | 3.1 |
| Completeness [%] | 96.8 | 95.1 |
| Redundancy | 5.09 | 5.14 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
