2J3G
L-ficolin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-04-19 |
Detector | ADSC CCD |
Spacegroup name | P 32 |
Unit cell lengths | 98.890, 98.890, 141.975 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.500 |
R-factor | 0.205 |
Rwork | 0.202 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jc9 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.335 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.690 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.090 |
Number of reflections | 52303 |
<I/σ(I)> | 7.8 |
Completeness [%] | 97.3 |
Redundancy | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |