2J2P
L-ficolin complexed to N-acetyl-cystein (150mM)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-02-11 |
Detector | ADSC CCD |
Spacegroup name | P 32 |
Unit cell lengths | 96.400, 96.400, 140.290 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.970 - 2.800 |
R-factor | 0.201 |
Rwork | 0.197 |
R-free | 0.27000 |
Structure solution method | OTHER |
RMSD bond length | 0.008 |
RMSD bond angle | 1.098 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.970 |
High resolution limit [Å] | 2.800 |
Rmerge | 0.130 |
Number of reflections | 33431 |
<I/σ(I)> | 6.3 |
Completeness [%] | 90.9 |
Redundancy | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |