2J1S
Structure of a Streptococcus pneumoniae fucose binding module in complex with fucose
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 43.523, 60.771, 99.499 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.500 |
| R-factor | 0.157 |
| Rwork | 0.155 |
| R-free | 0.19200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.640 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.550 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.040 | 0.250 |
| Number of reflections | 38029 | |
| <I/σ(I)> | 19.3 | 2.9 |
| Completeness [%] | 93.1 | 54.9 |
| Redundancy | 4 | 1.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
