2J1K

CAV-2 fibre head in complex with CAR D1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	I 4 2 2
Unit cell lengths	219.940, 219.940, 387.530
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	192.450 - 2.300
R-factor	0.172
Rwork	0.172
R-free	0.22000
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1kac
RMSD bond length	0.010
RMSD bond angle	1.248
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.700	2.380
High resolution limit [Å]	2.300	2.300
Rmerge	0.010	0.470
Number of reflections	200033
<I/σ(I)>	13.37	3.1
Completeness [%]	96.0	93
Redundancy	3.8	3.75

Crystallization Conditions

crystal ID	method	pH	temperature	details
1