2J12

Ad37 fibre head in complex with CAR D1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-3
Synchrotron site	ESRF
Beamline	ID14-3
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	I 2 3
Unit cell lengths	131.780, 131.780, 131.780
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	93.250 - 1.500
R-factor	0.149
Rwork	0.148
R-free	0.16900
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	PDB ENTRIES 1UXA 1kac
RMSD bond length	0.010
RMSD bond angle	1.309
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000
High resolution limit [Å]	1.500
Rmerge	0.070	0.400
Number of reflections	59884
Completeness [%]	99.0	90
Redundancy	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1