2J0Y
L-ficolin complexed to b-1,3-D-glucan
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-03-19 |
| Detector | ADSC CCD |
| Spacegroup name | P 32 |
| Unit cell lengths | 96.080, 96.080, 140.980 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.950 - 2.350 |
| R-factor | 0.198 |
| Rwork | 0.196 |
| R-free | 0.24200 |
| Structure solution method | OTHER |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.303 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.950 |
| High resolution limit [Å] | 2.350 |
| Rmerge | 0.090 |
| Number of reflections | 58888 |
| <I/σ(I)> | 12 |
| Completeness [%] | 98.1 |
| Redundancy | 4.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
