2J06
Crystal structure of the RasGAP SH3 domain at 1.8 Angstrom resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-05-19 |
Detector | ADSC CCD |
Spacegroup name | P 61 |
Unit cell lengths | 33.610, 33.610, 196.330 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.110 - 1.800 |
R-factor | 0.208 |
Rwork | 0.208 |
R-free | 0.24000 |
Structure solution method | SAD |
RMSD bond length | 0.027 |
RMSD bond angle | 3.400 |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.070 | 0.360 |
Number of reflections | 23136 | |
<I/σ(I)> | 21.8 | 4.9 |
Completeness [%] | 96.2 | 81.8 |
Redundancy | 4.9 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9 | 90 MM KNO3, 15.5% GLYCEROL, 90 MM TAPS, PH 9 AND 45.5% PEG8000 |